Lennie, A. R., Redfern, S. A. T., Schofield, P. F., Vaughan, D. J. (1995) Synthesis and Rietveld crystal structure refinement of mackinawite, tetragonal FeS. Mineralogical Magazine, 59 (397) 677-683 doi:10.1180/minmag.1995.059.397.10
| Reference Type | Journal (article/letter/editorial) | ||
|---|---|---|---|
| Title | Synthesis and Rietveld crystal structure refinement of mackinawite, tetragonal FeS | ||
| Journal | Mineralogical Magazine | ISSN | 0026-461X |
| Authors | Lennie, A. R. | Author | |
| Redfern, S. A. T. | Author | ||
| Schofield, P. F. | Author | ||
| Vaughan, D. J. | Author | ||
| Year | 1995 (December) | Volume | 59 |
| Issue | 397 | ||
| Publisher | Mineralogical Society | ||
| Download URL | https://rruff.info/doclib/MinMag/Volume_59/59-397-677.pdf+ | ||
| DOI | doi:10.1180/minmag.1995.059.397.10Search in ResearchGate | ||
| Generate Citation Formats | |||
| Mindat Ref. ID | 2697 | Long-form Identifier | mindat:1:5:2697:4 |
| GUID | 0 | ||
| Full Reference | Lennie, A. R., Redfern, S. A. T., Schofield, P. F., Vaughan, D. J. (1995) Synthesis and Rietveld crystal structure refinement of mackinawite, tetragonal FeS. Mineralogical Magazine, 59 (397) 677-683 doi:10.1180/minmag.1995.059.397.10 | ||
| Plain Text | Lennie, A. R., Redfern, S. A. T., Schofield, P. F., Vaughan, D. J. (1995) Synthesis and Rietveld crystal structure refinement of mackinawite, tetragonal FeS. Mineralogical Magazine, 59 (397) 677-683 doi:10.1180/minmag.1995.059.397.10 | ||
| In | (1995, December) Mineralogical Magazine Vol. 59 (397) Mineralogical Society | ||
| Abstract/Notes | AbstractMackinawite, tetragonal FeS, has been synthesised by reacting iron with Na2S solutions. A Rietveld structure refinement of X-ray powder diffraction data, recorded using X-rays monochromated from synchrotron radiation with a wavelength of 0.6023 Ã…, has been performed. The structure has been refined in the tetragonal space group, P4/nmm, and has the following cell parameters: a = 3.6735(4), c = 5.0328(7) Ã…, V = 67.914(24) Ã…3. Our refinement shows that the FeS4 tetrahedron in mackinawite is almost perfectly regular, with a much smaller distortion than has been previously reported. An improved X-ray diffraction data set is provided. | ||
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